ST10

On-site Fuel Stability and Compatibility Tester
ASTM D4740


 Download the brochure

Patent(s) :
U.S. Pat. No. 15/830,247


Bulk fuel stored for long periods can become unstable the asphaltene content can precipitate out of solution causing the formation of sludge. This has the potential to block filters and pipes, leaving tanks with an unpumpable residue.

The 'break up' is dependent on the nature of the liquid hydrocarbons in which the asphaltenes are suspended. If the medium is aromatic (hydrocarbons in ring formation) then they will remain in suspension but if it is paraffinic (linear hydrocarbon formation) the asphaltenes may have a propensity to coalesce into sludge. Once a fuel has chemically broken down there is no way to satisfactorily reverse the process. Precipitated asphaltene cannot be re-dissolved.

Although incompatibility is not a common phenomenon its likelihood increases in tandem with fuel switching, such as when entering and leaving an ECA. Compatibility problems must be treated as a critical concern as it can result in power failure, fuel systems can become paralyzed and the work for cleaning up the results is both difficult and time consuming. It is important to remember that a stable fuel oil can become unstable when mixed with another stable grade although generally fuels of the same viscosity grade with similar densities will be compatible.

The marine fuel market is undergoing complex and far-reaching change, largely as a result of a growing body of environmental legislation. Issues surrounding fuel stability and compatibility have never been more relevant, especially with the new 0.10 per cent sulphur level for fuels used in Emission Control Areas (ECAs).

 

On board a vessel, a good way to measure the compatibility of marine fuels, including residual and distillate fuels, is the ASTM D4740 spot test. The ideal percentage mix is 50/50 as this is the worst case scenario.

A drop of the blend is put on a test paper and heated to 100°C. After 1 hour, the test paper is removed from the oven and the resultant spot is examined for evidence of precipitation and rated for compatibility against D4740 reference spots.

AD Systems has developed a portable / on-site / on-boardfully automated instrument for stability and compatibility testing of heavy fuel oil. This portable device is a complete automation of the ASTM D4740 method.

This method is very simple and practical for the test but it had the serious handicap to rely on the know-how and subjectivity of the operator.

We have grouped all the phases of the test in a suitcase, the conditioning of the samples, and the preparation of the spot, its drying and the automatic rating by camera and associated software.

The only phases under the load of the operator are the sampling and the deposition of the drop with the aid of a micropipette supplied with the equipment.

As a result, the apparatus can be used anywhere by untrained persons for this test whenever power is available.

The apparatus is provided with a database for storing the results. The image of the spot is memorized at the time the spot is rated and we therefore ensure perfect traceability of the test.


OCM
Pipeline and terminals

  • A complete automated system self-contained in a carrying case
  • Multi-applications instrument, lab, on-site, on-board
    • Vessel operators
    • Refineries
    • Terminals
    • Power plants
    • Independent laboratories
    • Military
  • Standard test method used by conventional laboratories.
  • Fully automated, no training or analytical knowledge required
  • Removes subjectivity
  • Prevent sludge deposits, failure of fuel handling systems and costly combustion related engine damage.
  • No solvents
  • Quick and reliable determination.
  • Designed for both on-board use and lab use.
  • Full traceability with built-in database


The sample is prepared according to the procedure described in the ASTM D4740 test method. Once the fuel is dropped on the filter paper, all phases are automatically performed. A picture of the spot is taken after the one hour drying phase. The picture is binarized and the ST10 reports a 1 to 5 rating depending on the stability of the fuel.

  • The ST10 comprises:
  • All consumables and accessories including micropipette
  • Built- oven for sample and filter paper
  • Automatic handling of the filter paper
  • CCD camera to take the sample spot picture
  • A built-in computer
  • A dedicated software to analyze the picture and report the result
  • A built-in database for full test traceability
  • USB et Ethernet ports

  • The operator keys in all information related to the sample and the test conditions
  • The fuel or the mixed fuel is poured into a disposable vial and then placed into the built-in oven.
  • The filter paper is positioned on the conveyor. The ST10 automatically places the filter paper in the oven for drying at 100°C.
  • The operator is prompted when the sample temperature is reached and the filter paper is pre-positionedfor sampleinjection.
  • With the micropipette, the operator pours one drop of fuel on the filter paper.
  • The fuel spot is automatically positioned in the oven at 100°C.
  • After the drying phase, the fuel spot is automatically moved under the camera and a picture is captured.
  • The software analyses the fuel spot.
  • The test result is displayed and stored in a built-in database.


The test result is displayed and saved in the built-in database with all test conditions including the spot image.

List of parameters saved with a result : 

  • Sample type(s)
  • Sample ID(s)
  • ASTM D4740 rating (from 1 to 5)
  • Date & time
  • Operator name
  • Comments
  • Test conditions
  • Calibration information (tube serial number + date of calibration)
  • Instrument serial number
  • Software version

 

The results can be displayed, memorized on a USB disk on key or send to a LIMS via the LAN connection


Reported Results Measurement Range
ASTM D4740 rating From 1 to 5
Accuracy Less than one rating
Test mode Programmable:
  • Fuel Stability
  • Fuel Compatibility
Technical Specification Description
Display 7" Touchscreen
10 finger capacitive touch
Screensize : 155mm x 86mm
Resolution : 800 x 480 px
Oven temperature 100°C for the filter paper
93°C for the fuel
Resolution 0.1°C, precision ±0.2°C
Sample heating time According to D4740 or programmable in minutes
Oil spot drying time According to D4740 or programmable in minutes
Parameters saved with a test result Stability or Compatiblity (1 to 5)
Fuel spot image
Test mode
Fuel heating time
Spot drying time
Sample type
Sample ID
Date & Time
Operator Name
Comments
Software version
Results storage Up to 100 000 results
LAN connectivity Ethernet port RJ45
Data output USB(4), Ethernet
Dimensions W x D x H (mm)       W x D x H (inches)
420 x 350 x 220       16.5"x 14"x 8.5"
Weight 9kg (20lbs)
Electrical 115 to 230V - 2A - 50/60Hz

The Instrument
Catalog Number Description Picture
AA120-001 On-site Fuel Stability and Compatibility Tester - ST10 according to ASTM D4740 
Electrical: 110/240 VAC, 2A, 50/60Hz, User manual in English
Software option
Catalog Number Description Picture
AK120-001 Optional software for Lubricant Dispersancy Testing - ST10
Accessories
Catalog Number Description Picture
AC120-001 Pack of 100 Whatman filter paper diam. 42.5 mm
AC120-002 Pack of 200 disposable 15 mL vials
AC000-003 Disposabletips for 25 µL micropipette / pack of 200